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Example sentences for: nmr
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The likelihood that this is correct is accentuated by the fact that Taxol conformational analysis by NMR has never been performed in pure water, but always as a mixture of DMSO-d 6 and D 2 O. [ 5 ] In addition, in anhydrous methanol, a solvent with a high dielectric and the capacity for explicit hydrogen bonding as in water, the polar form goes undetected.
The claim that such turbidity did not affect 13C-NMR measurements [ 3 5 6 ] contrasts with evidence that even small multimers can change NMR chemical shifts [ 25 26 ] . It should be noted also that, at high concentrations of B =, extensive, reversible self-association of B =can lead to apparently stable supersaturation with no separation of an insoluble phase [ 2 ] . For example, at pH 8.5 and a UCB concentration of 20 μM (63 times S), the weight-average aggregation number of UCB has been found to be 7.17 [ 18 ] , corresponding to a molecular weight of 4,195.
The single crystal X-ray structure [ 14 ] and the 2-D NMR (CDCl 3 ) [ 6d ] of Taxotere likewise demonstrate hydrophobic association, in this case between the tert -butyl and the C2 phenyl group.
Target sequences related to proteins that have conformations determined by experiment (X-ray crystallography or NMR) were candidates for comparative modelling.
Figure 4shows those positions in the N-terminal PH domain of pleckstrin that have been implicated, based on NMR analysis, to contact PIP 2 [ 17 ] . Boi1's PH domain has identical or similar amino acids at most of the analogous positions (Fig.
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